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A depolymerizable vitrimer that allows both reprocessability and monomer recovery by a simple and scalable one‐pot two‐step synthesis of vitrimers from cyclic lactones is reported. Biobased δ‐valerolactone with alkyl substituents (δ‐lactone) has low ceiling temperature; thus, their ring‐opening‐polymerized aliphatic polyesters are capable of depolymerizing back to monomers. In this work, the amorphous...
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