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A dynamic acetonitrile | aqueous electrolyte phase boundary in contact with platinised Teflon working electrodes is investigated. High concentrations of salt in the aqueous phase (2M NaCl and 0.1M NaClO 4 ) ensure immiscibility and the polar nature of acetonitrile aids the formation of a well-behaved triple phase boundary reaction zone. The one-electron oxidation of tert-butylferrocene in...
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