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There has been speculations on the structures of TiF 4 polymeric complexes {TiF 4 L} n (L=molecular donor) for several decades, however no structurally characterized examples have been reported. In this work the complex {TiF 4 (PhCN)} 3 was isolated from a solution of TiF 4 in PhCN (donor number DN=11.9kcalmol −1 ) as well as from the mixtures...
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