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Phosphate ester bonds are widely present in nature (e. g. DNA/RNA) and can be extremely stable against hydrolysis without the help of catalysts. Previously, we showed how the combination of phosphoryl and calix[4]arene moieties in the same organic framework (LPO) allows isolation of single lanthanide (Ln) metal ions as [LnIII(LPO)2](O3SCF3)3. Here we report how by controlling the reaction conditions...
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