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The clathrate‐I Ba8–xSi46 was manufactured from BaSi2 and α‐Si by high‐pressure high‐temperature synthesis at 5 GPa and 900 °C and by redox reaction from Ba4Li2Si6. The transport properties were measured on specimens from the high‐pressure high‐temperature synthesis. The composition of the Ba8–xSi46 phase [space group Pm$\bar{3}$n, a = 10.3051(1) Å] corresponds to x = 0.8(2) according to the refined...
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