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The title compounds are obtained in high yield from stoichiometric mixtures of Ln, LnI 3 and graphite, heated at 900–950°C in welded Ta containers. The crystal structures of new Pr and Nd phases determined by single-crystal X-ray diffraction are related to those of other Ln 12 (C 2 ) 3 I 17 -type compounds (C 2/c, a=19.610(1) and 19.574(4)Å, b=12.406(2) and...
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