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Controllable synthesis of large domain, high‐quality monolayer MoS2 is the basic premise both for exploring some fundamental physical issues, and for engineering its applications in nanoelectronics, optoelectronics, etc. Herein, by introducing H2 as carrier gas, the successful synthesis of large domain monolayer MoS2 triangular flakes on Au foils, with the edge length approaching to 80 mm is reported...
Q. Fu, Y. Zhang, and co‐workers identify the crystal orientations and domain boundaries of MoS2 flakes directly on Au foils on page 842 by using low‐energy electron microscopy/diffraction for the first time. These transfer‐free characterizations should shed light on the initial growth and the aggregation of MoS2.
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