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The first synthetic study on PbBiO2Cl/BiOCl nanocomposite preparation using a controlled hydrothermal method is reported. The composition and morphologies of the samples could be controlled by adjusting some growth parameters, including reaction pH, Pb/Bi molar ratio, and temperature. All the samples are characterized by XRD, TEM, XPS, SEM-EDS, FT-IR, BET, EPR, and UV–vis-DRS. The photodegradation...
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