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Novel thermosets were prepared by the base‐catalysed reaction between a cycloaliphatic resin (ECC) and various thiol crosslinkers. 4‐(N,N‐Dimethylaminopyridine) (DMAP) was used as base catalyst for the thiol–epoxy reaction. A commercial tetrathiol (PETMP) and three different thiols synthesized by us, 6SH‐SQ, 3SH‐EU and 3SH‐ISO, were tested. 6SH‐SQ and 3SH‐EU were prepared from vinyl or allyl compounds...
A new allyl terminated hyperbranched poly(ethyleneimine) was synthesized and characterized and then used in different proportions as multifunctional macromonomer in tetrathiol–diglycidyl ether of bisphenol A formulations. The curing process had a two-stage character and was composed by two click reactions: a first photoinduced thiol–ene addition followed by a thermal thiol–epoxy reaction. The thiol–ene...
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