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Titania nanotube array with an enlarged tube diameter of 110nm and length of 700nm was grown on titanium metal by a potentiostatic anodization in hydrofluoric acid–phosphoric acid–ethenyl glycol electrolyte. Nickel hydroxide was introduced into this titania nanotubes by either an electrodeposition–oxidation or hydrothermal process. Nickel oxide–titania composite was finally formed by heating treatment...
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