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Abstract. A simple and rapid electrochemical method to detect the hydroxyl radical is described. This method employed the reaction between OH and dimethyl sulfoxide (DMSO) to generate quantitatively formaldehyde, which then reacted with hydrazine hydrochloride at pH 6.2. The product showed a second-order derivative cathodic wave with the peak potential of 1.08V( vs SCE) by single sweep oscillopolarography...
. A simple and rapid electrochemical method to detect the hydroxyl radical is described. This method employed the reaction between ·OH and dimethyl sulfoxide (DMSO) to generate quantitatively formaldehyde, which then reacted with hydrazine hydrochloride at pH 6.2. The product showed a second-order derivative cathodic wave with the peak potential of –1.08 V( vs SCE) by single sweep oscillopolarography...
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