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Alkaline metal (AM) atoms filled CoSb3 skutterudites are synthesized by melting method and sintered by spark plasma sintering. The maximal filling fraction or filling fraction limit (FFL) of AM (AM=Li, Na, K, Cs) in CoSb3 are estimated experimentally and show good agreement with our previous calculations based on density functional method. The effect of thermodynamics properties on FFL, crystallographic...
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