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An iridium(III) complex comprising three different cyclometalated phenylpyridine‐based ligands was designed and synthesized. Interestingly, mixed‐ligand complexes could be obtained by using a simple and straightforward procedure. A tris(heteroleptic) IrIII complex was obtained as a mixture of stereoisomers that could not be separated. Photophysical properties of the tris(heteroleptic) complex was...
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