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2D metal–organic nanosheets (MONs), akin to graphene, have aroused immense contemporary interest. In our quest to develop functional 2D MONs based on organic linkers designed de novo, we reasoned that benzene‐tetrabenzoic acid, which has been exploited tremendously in the construction of pillared metal–organic frameworks (MOFs), could be maneuvered readily to access redox‐active MONs based on the...
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