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A new polycation‐type phosphate of H{[Na(H2O)3]6F}(PO4)2 ⋅ 2(H2O) (FNPO) was synthesized by a mild hydrothermal method. FNPO crystallizes in the cubic space group of
with cell parameters of a=27.778 Å and Z=32. In the structure of FNPO, every sodium ion is six‐fold coordinated to five water molecules and one fluoride ion in forming electroneutral [NaF(H2O)5] octahedra, while one kind of super...
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