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Olivine-type Li rich Li1+xFePO4/C composites are synthesized by a solid state reaction process using premilled Li2CO3 and pre-synthesized amorphous FePO4·xH2O powders. The amorphous FePO4·xH2O powders are prepared from an industrial waste liquid (by-product), a FeCl3 (38%) solution, via a precipitation process. In addition, lithium carbonate is pre-milled using a high energy nano mill to control particle...
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