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Transition metal osmium borides were synthesized by mechanochemical method using high‐energy ball‐milling with Os (Osmium) and B (Boron) powders as raw materials. The formation process, reaction mechanism, and thermal stability of the mechochemically synthesized osmium borides were studied. Almost pure Os2B3 phase was obtained when the Os‐to‐B molar ratio was 1:2; while ReB2‐type hexagonal OsB2 with...
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