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The formation of dual‐component organic nanoparticles by a modified emulsion‐templated freeze‐drying approach leads to aqueous nanosuspensions showing fluorescence (Förster) resonance energy transfer (FRET) from within a distribution of single nanoparticles. The combination of both FRET dyes within dual‐component nanoparticles (<200 nm) allows the spatial and physical monitoring of the particles,...
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