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Inorganic–organic boron–silicon–acetylene hybrid polymer (PABS) was prepared by the polycondensation reaction between phenylboric acid and diphenyldichlorosilane and then terminated by phenylacetylene. The structure was characterized by using FTIR, 13C‐NMR, 1H‐NMR, and GPC. PABS was a kind of resin exhibited high viscous at room temperature and good solubility in common organic solvents. The thermal...
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