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Rhodium(III) and ruthenium(II) complexes supported by a pentadentate tetrapodal (pentaPod) phosphine ligand are synthesized through abstraction of one chloride ligand from initially obtained κ4‐pentaPod coordinated dichloro complexes [MCl2(κ4‐P2MePP2Ph)]+/0 (M=Rh(III), Ru(II)) with alkali salts of weakly coordinating anions. While for the rhodium κ5‐pentaPod complex the remaining, axial chloride ligand...
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