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Nanothermometers that can reflect temperature in real‐time are crucial for photothermal therapy. Near‐infrared (NIR) fluorescent probes that conform to Boltzmann distribution will play an important role if they have the above characteristics. Here, the LiLuF4: Nd3+/Yb3+ nanocrystals were designed and synthesized by control, exhibiting multiple bright near‐infrared emission peaks at 925–1080 nm region...
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