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Carbamazepine is separated from 10,11-dihydrocarbamazepine and other impurities using a solution of sodium tetraborate decahydrate (12.5 mmol/l) and sodium dodecyl sulfate (50 mmol/l) in water-methanol (9:1, w/w; apparent pH 9.2). This method is optimised with regard to concentration of the organic modifier, temperature and voltage. The influence of the capillary type and the instrumentation has...
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