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Herein, a series of 1,2‐disubstituted 3,3,4,4,5,5‐hexafluorocyclopentene derivatives is synthesized from the commercially available octafluorocyclopentene via addition‐elimination reactions, and their photophysical properties are investigated in detail. 1,2‐Bis[2‐(4‐alkoxyaryl)ethyn‐1‐yl]‐3,3,4,4,5,5‐hexafluorocyclopentene exhibits UV‐absorption at 345 nm in CH2Cl2 and deep blue photoluminescence...
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