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The rhodium(III)‐catalyzed C−H amidation and subsequent C−N bond formation reaction of indolines with aryl and alkyl isocyanates at room temperature are reported. These transformations allow the generation of N‐aroylurea functionality at the C7‐position of indolines, which is known as a crucial scaffold found in biologically active molecules. In addition, the synthesis of pyrroloindolidione derivatives...
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