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The electrocatalytic reduction of benzyl bromide at a silver cathode has been investigated in acetonitrile in the absence and presence of acids, using cyclic voltammetry (CV) and controlled-potential electrolysis (CPE). CV gives rise to two reduction waves, which represent the dissociative 1e − reduction of PhCH 2 Br to PhCH2 and Br − followed by a further reduction of the...
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