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The quaternary tantalum thiophosphates K 0.38 TaPS 6 (1) and Rb 0.46 TaPS 6 (2) were synthesized by reacting TaS 2 with an in situ formed melt of A 2 S 3 (A = K, Rb), P 2 S 5 and S. Both structures are related to the basic tunnel structures of the known ternary compounds TaPS 6 and Ta 4 P 4 S 29 ...
The new quaternary tantalum thiophosphate Rb 4 Ta 4 P 4 S 24 was synthesized by reacting TaS 2 with a molten polythiophosphate flux formed by Rb 2 S 3 , P 2 S 5 and S at 773 K. The compound crystallizes in the monoclinic space group P2 1 /n with a=13.849(3), b=17.647(4), c=15.900(3) A, β=106.81(3) o , V=3720...
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