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Neutral π-stacked metallomacrocycle was prepared using fac-Re(CO) 3 , and linear ditopic π-conjugated nitrogen donors in water–toluene mixture under reflux condition. Two ethylene units in the cycle are parallel to each other with a distance of 3.4Å, which undergo topochemical conformational change from a parallel conformation to criss-cross conformation and photoreduction under UV-light irradiation...
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