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Photoinduced debenzylations of phenylalanine and tyrosine derivatives with dicyanoarenes afford glycine derivatives by the generation of radical cations. Despite the limited substrate scope, the radical cation of phenylalanine and tyrosine derivatives bearing both a carbamate (without an aromatic group) at the N-terminal and an amide at the C-terminal could promote the breaking C–C bond at the benzylic...
A glycosyl phosphatidylinositol, 2,6-di-O-α-d-mannopyranosylphosphatidyl-d-myo-inositol was synthesized in a regiospecific manner via a key intermediate, 1,2-O-cyclohexylidene-3,4-O-(tetraisopropyldisiloxane-1,3-diyl)-myo -inositol. In the glycosylation, mannopyranosyl phosphite proved to be useful as a glycosyl donor.
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