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The oxonitridoberyllate Eu3Be22N16O was synthesized from Eu(NH2)2, Be3N2 and BeO in a W crucible under N2 atmosphere in a radio‐frequency furnace at 1400 °C. The crystal structure was solved and refined from X‐ray diffraction data (C2/c (no. 15), a=20.620(2), b=8.722(6), c=17.506(2) Å, β=120.782(3)°) and confirmed with Rietveld refinement methods as well as lattice‐energy calculations (Madelung part...
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