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Herein, we report the preparation of a new unsymmetrical, bis(thiophosphinoyl)‐substituted dilithio methandiide and its application for the synthesis of zirconium‐ and palladium‐carbene complexes. These complexes were found to exhibit remarkably shielded 13C NMR shifts, which are much more highfield‐shifted than those of “normal” carbene complexes. DFT calculations were performed to determine the...
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