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3-Furaldehyde thiosemicarbazone (3FTSC) and 3-(2-furyl)prop-2-enal thiosemicarbazone (FATSC) have been prepared, their structures solved and IR, 1 H NMR spectra recorded. The thiosemicarbazone moiety in both compounds shows an E configuration about C1–N2 and C2–N3. Intramolecular and intermolecular hydrogen bondings occur in both the molecules. The angles between the mean planes of the furanic...
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