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Here we provide evidence that the formation of PuO2 nanoparticles from oxidized PuVI under alkaline conditions proceeds through the formation of an intermediate PuV solid phase, similar to NH4PuO2CO3, which is stable over a period of several months. For the first time, state‐of‐the‐art experiments at Pu M4 and at L3 absorption edges combined with theoretical calculations unambiguously allow to determine...
Eine neuartige feste Phase von fünfwertigem Plutonium wurde auf dem Reaktionspfad von wässrigem PuVI zu PuO2‐Nanopartikeln beobachtet, wie K. O. Kvashnina et al. in ihrer Zuschrift auf S. 17722 berichten. Erreicht wurde dies durch die Kombination aus einer Fluoreszenzdetektion mit hoher Energieauflösung an den M4‐ und L3‐Kanten von Pu und Berechnungen der Elektronenstruktur.
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