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An efficient NiSx‐modified β‐Ni(OH)2 electrode is reported for the selective oxidation reaction of 5‐hydroxymethylfurfural (HMFOR) with excellent electrocatalytic 5‐hydroxymethylfurfural (HMF) selectivity (99.4%), conversion (97.7%), and Faradaic efficiency (98.3%). The decoration of NiSx will evoke high‐valence Ni2+δ species in the reconstructed β‐Ni(OH)2 electrode, which are the real active species...
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