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The dehydrocoupling/dehydrogenation behavior of primary arylamine–borane adducts ArNH2⋅BH3 (3 a–c; Ar=a: Ph, b: p‐MeOC6H4, c: p‐CF3C6H4) has been studied in detail both in solution at ambient temperature as well as in the solid state at ambient or elevated temperatures. The presence of a metal catalyst was found to be unnecessary for the release of H2. From reactions of 3 a,b in concentrated solutions...
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