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A group of new polymolybdates was synthesized and tested in the catalytic oxidation of cycloalkanes. Investigated compounds exhibit broad structural diversity including polymolybdates with isolated anionic clusters (0-dim), polymeric anions (1-dim), Mo–O layers (2-dim) as well as hexagonal and orthorhombic molybdenum oxides (3-dim). All studied molybdenum complexes were found to be active in the reaction...
Three new oxodiperoxomolybdenum complexes with nicotinic acid have been synthesized and characterized with the use of single-crystal analysis, XRPD versus temperature, TG/DSC, SEM and IR spectroscopy. The investigated compounds are: 1 – (NH 4 ) 2 ·[MoO(O 2 ) 2 .N-nicO] 2 , 2 – (nicH) 2 ·[MoO(O 2 ) 2 .N-nicO] 2 ·2(H 2 O),...
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