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We present an extension of a previously published work (J. Solid State Chem. 181 (2008) 3229) concerning Metal-Organic Frameworks (MOFs) of general formula Ni5(OH)6(CnH2n−4O4)2. A modified synthesis procedure comprising a room-temperature step prior to the hydrothermal treatment was employed. This preliminary step made use of peristaltic pumps allowing slow mixing of the reactants at a constant pH...
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