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It is apparent that coordinatively unsaturated transition complexes can catalyze hydrogen production from acid or water via metal-hydride intermediates. To test if coordinatively saturated complexes can also act as electrocatalysts for hydrogen evolution, two electrocatalytic systems based on coordinatively saturated metal-1,10-phenanthroline (phen) complexes, [MII(phen)3](PCPP)2 (PCPP = pentacyanopropenide;...
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