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Novel Covalent organic skeleton/metal oxide (COF/MOx; M = Ti, Zn, Zr, Sn, Ce, Nb) Z scheme heterojunction is constructed to achieve highly selective oxidation of nitric oxide (NO). Under visible‐light irradiation, the optimized COF/TiO2 (CF/TS0.05) catalyst showed an excellent NO removal rate (64.5%), resulting from the improvement of light absorption performance, the separation efficiency of photoexcited...