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A systematic series of four novel homo‐ and heteroleptic CuI photosensitizers based on tetradentate 1,10‐phenanthroline ligands of the type X^N^N^X containing two additional donor moieties in the 2,9‐position (X=SMe or OMe) were designed. Their solid‐state structures were assessed by X‐ray diffraction. Cyclic voltammetry, UV‐vis absorption, emission and X‐ray absorption spectroscopy were then used...
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