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The synthesis, structure, and chromogenic properties of polymethylene-vaulted trans-bis(salicylaldiminato)palladium(II) complexes are described. A series of the Pd complexes incorporating nona-, deca-, undeca- and dodecamethylene bridges (1a: n=9; 1b: n=10; 1c: n=11; 1d: n=12) was prepared by the treatment of Pd(OAc)2 with the corresponding N,N′-bis(salicylidene)-1,ω-alkanediamines. The trans-coordination,...
The synthesis, structure, and flapping motion of clothespin‐shaped binuclear trans‐bis(salicylaldiminato)palladium(II) complexes (anti‐1) with 4‐azaheptamethylene linkers bearing amide (a–g), urethane (h), or urea (i) functionalities are described in this report. Various 2D 1H NMR experiments and XRD analyses indicate that the amide‐ and urethane‐linked anti‐1 a,b,d–h complexes exist as equilibrated...
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