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Thermal decomposition of cesium azide (CsN3) leaves elemental cesium behind, which was in‐situ produced and used for the syntheses of the two new cesium thiotellurates Cs2[TeS2] and Cs2[TeS3] along with appropriate amounts of tellurium and sulfur. The first compound crystallizes orthorhombically in space group Cmc21 with the lattice parameters a = 783.39(4), b = 1126.72(8), c = 823.04(5) pm (Z = 4)...
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