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Alkalimetallsalze des Typs M+[Ter(iPr)P−C(=S)−P(iPr)2S].− (M=Na, K; 2_M; Ter=2,6‐bis‐(2,4,6‐trimethylphenyl)phenyl) mit einem raumtemperaturstabilen Thioketylradikalanion wurden durch die Reduktion des Thioketons Ter(iPr)P−C(=S)−P(iPr)2S (1) mit Alkalimetallen (Na, K) erhalten. Einkristall‐Röntgenstrukturanalyse sowie ESR‐Spektroskopie konnten das Vorliegen des Thioketylradikalanions sowohl im Festkörper...
Fluorinated organic compounds are gaining increasing interest for life science applications. The replacement of hydrogen in arenes or heteroarenes by a perfluoroalkyl group has a profound influence on the physical and biological properties of such building blocks. Here, an operationally simple protocol for the direct CH perfluoroalkylation of (hetero)arenes with RfI or RfBr has been developed, using...
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