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The design and synthesis of faceted nanoparticles with a controlled composition is of enormous importance to modern catalyst engineering. Faceted FePt‐Fe3O4 dumbbell nanoparticles are prepared by a simple, one‐pot technique that avoids the need for expensive additives or preformed seeds. The faceted product consists of an FePt octopod and a cubic Fe3O4 lobe, of mean diameter 13.6 and 14.9 nm, respectively...
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