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Chemically inert oxidometal(V) corrols of molybdenum and rhenium undergo clean ligand‐exchange reactions upon the action of SiCl4. The resulting dichlorido complexes show trigonal prismatic coordination of the metal ion with the chlorine atoms residing in a cis configuration, and were studied by optical and resonance spectroscopy as well as DFT calculations. In situ reactivity studies with carbon...
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