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Incorporating nanoscale Si into a carbon matrix with high dispersity is desirable for the preparation of lithium‐ion batteries (LIBs) but remains challenging. A space‐confined catalytic strategy is proposed for direct superassembly of Si nanodots within a carbon (Si NDs⊂C) framework by copyrolysis of triphenyltin hydride (TPT) and diphenylsilane (DPS), where Sn atomic clusters created from TPT pyrolysis...
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