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Enantioselective trichloromethylation of Morita–Baylis–Hillman (MBH)‐type allylic fluorides with chloroform (HCCl3) under organocatalysis was achieved with high to excellent enantioselectivities. Silicon‐assisted C−F bond activation by a Ruppert–Prakash reagent and direct activation of HCCl3 by a carbanion exchange process with trifluoromethyl (CF3) carbanion generated in situ from the Ruppert‐Prakash...
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