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A Sn‐phony in B! BN isosteres of biphenyl compounds are prepared through Rh‐catalyzed cross‐coupling between 2‐chloro‐1,2‐azaborines and arylstannanes (see scheme). The synthetic method should enable investigations of structure–activity relationships (SARs) by expanding the chemical space of the pharmaceutically relevant biphenyl structure through BN/CC isosterism.
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