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The homogeneity range of ternary iron indium thiospinel at 873 K was investigated. A detailed study was focused on two distinct series (y=z): 1) a previously reported charge‐balanced (In0.67+0.33y□0.33−0.33y)tetr[In2−zFez]octS4 (A1‐series; □ stands for vacancy; the abbreviations “tetr” and “oct” indicate atoms occupying tetrahedral 8a and octahedral 16d sites, respectively) and 2) a new charge‐unbalanced...
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