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We report on the first thoroughly characterized molybdenum borate, which was synthesized in a high‐pressure/high‐temperature experiment at 12.3 GPa/1300 °C using a Walker‐type multianvil apparatus. Mo2B4O9 incorporates tetrahedral molybdenum clusters into an anionic borate crystal structure—a structural motif that has never been observed before in the wide field of borate crystal chemistry. The six...
Mo2B4O9vereint zwei Forschungsfelder – Boratchemie und Metallcluster –, denn es ist das erste Borat, das Übergangsmetallcluster in der Kristallstruktur enthält. Wie H. Huppertz und Mitarbeiter in ihrer Zuschrift auf S. 6549 zeigen, ebnete ein gezielter Reduktionsprozess in einem Hochdruckexperiment den Weg zu dieser neuen Substanzklasse.
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