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Enhancing photoluminescence quantum yield (PLQY) is one of the most important issues in photoluminescent materials. Herein, a molecule design strategy to improve the PLQY in 0D metal halides is proposed. Two new lead‐free organic–inorganic metal halide hybrids with broadband orange emissions have been prepared with a PLQY increase of 57% from (C6N2H16)SbCl5 (I) to (C6N2H16)SbCl5⋅H2O (II) by introducing...
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